1546 - 2226 ( on - line ) Editors - In - Chief : Surya Kalidindi N . Ramakrishnan Raimund Rolfes Vinod Tewary Honorary

We have measured and reconstructed via forward modeling a small volume of microstructure of high purity, well annealed nickel using high energy xray diffraction microscopy (HEDM). Statistical distributions characterizing grain orientations, intra-granular misorientations, and nearest neighbor grain misorientations are extracted. Results are consistent with recent electron backscatter diffraction measurements. Peaks in the grain neighbor misorientation angle distribution at 60 degrees (Σ3) and 39 degrees (Σ9) have resolution limited widths of ≈ 0.14 degree FWHM. The analysis demonstrates that HEDM can recover grain and grain boundary statistics comparable to OIM volume measurements; more extensive data sets will lead to full, five parameter grain boundary character distributions. Due to its non-destructive nature, HEDM can then watch, both statistically and through tracking of individual grains and boundaries, the evolution of such distributions with processing of the sample.